In-situ Raman Electrochemical Cell Assembly

Captions

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1. Start by assembling the Working Electrode. 
   
2. Insert the Working Electrode Holder with an O-ring
   
3. Loosen the screw and carefully attach the Working Electrode (WE).  
   
4. You can attach a WE of your choice. Normal, SERS, SHINERS 
   
5. Rotate the WE to position it closer to the Window. Make sure active material is coated on this side 
   
6. Secure the Electrode properly 
   
7. Specially designed Detachable L-shaped Glassy Carbon will also fit into the cell  
   
8. Need to Purchase Separately (C2040A1)  
   
9. L-shape design helps to reduce distortions by reducing the Gap between the WE and the Window 
   



10. You can attach the Reference and Counter Electrodes next
11. Adjust the O-ring to make the Reference Electrode positions well 
    
12. Use similar technique to position the Counter Electrode well 
    
13. Let’s attach the gas line now 
    
14. Use 3 mm inner diameter gas feedthrough screws to secure the line  
    
15. Recommended to use the lower port as the Gas Inlet  
    
16. Upper one as the Gas Outlet 
    
17. Push-fit connectors are provided to extend the gas tubing towards Swagelok fittings or Gas Analysis Chambers 
    
18. Let’s fit the Optical Window now  - Gaskets with different thickness are provided allowing users to adjust the distance between the electrode and the Optical Window
    
19. Remove the PTFE Cap. Use the tool provided if too tight 
    
20. Place the gasket (Peel off the cover when you do it) 
    
21. You can fill up the electrolyte now before fitting the Optical window  
    
22. Place the Optical Window now. Quartz provided with the package 
    
23. Tighten the Lid 
    
24. Now you are ready to start your experiment 
    
25. Additional port is provided on the side. You can use it for sampling, temperature probing, gas purging, etc 
    
26. Contact Us through the product page or support@ossila.com for further support

What's Included

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The standard items included with the C2035R1 In-situ Raman Electrochemical Cell in the assembly video above are the following

• 1 x PTFE cell
• 1 x PEEK platinum sheet electrode holder
  
• 1 x φ0.5*37mm platinum wire electrode
• 1 x φ6mm silver chloride reference electrode
• 1 x suction cup
• 1 x Nylon hand screw accessories
• 1 x PTFE tube φ3mm
• 2 x φ3mm PU quick connect
• 5 x φ41*1mm quartz light window
• 8 x light window sealing fluorine rubber gasket
• 6 x electrode hole sealing screw
• 4 x gas hole sealing screw

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