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Sealed Micro-Electrochemical Cell Setup

Captions


  1. How to assemble the 10 ml cells with three electrode ports and two gas inlet/outlets
  2. The Sealed Micro-Electrocemical Cell with Sampling Window (C2031W1) has an additional sampling window
  3. Let’s quickly see how to assemble. (Electrodes need to be purchased separately)
  4. For the working electrode, you can use an Electrode Holder or a Disk Electrode with the cell
  5. Fix Working Electrode
  6. Platinum and glassy carbon standard disk and removable disk working electrodes are available to purchase. 
  7. Platinum electrode holders and glassy carbon electrode holders are available to purchase
  8. Fix Reference Electrode
  9. Ag/AgCl for Aqueous and Ag/Ag+ for non-aqueous
  10. Allow the reference electrode the reach the equilibrium once fills with the solution before use
  11. Always makes sure to use the provided O-rings to achieve adequate sealing
  12. Fix Counter Electrode
  13. Wire and Coil Counter/ Auxiliary Electrodes fits well with the cell
  14. Can fix the gas inlet/outlets or close the ports with stoppers (provided) as required 
  15. Follow the steps to obtain good sealing
  16. Let’s set up the sampling window
  17. Place the silicone disk seal 
  18. Tighten the sampling window screw
  19. Syringe tip is provided to collect gas or liquid samples within the cell
  20. Now your cell is ready
  21. Around 3ml minimum electrolyte is needed to immerse the electrodes
  22. Electrodes are well immersed in the 5 ml electrolyte
  23. The cell has maximum 10-12 ml capacity
  24. Spare parts and additional accessories include
    • Sampling Window and O-rings
    • Electrode Fixing Screws and O-rings
    • O-rings for PTFE Lid
    • Syringe Needle
    • PTFE Tubing (1m)
    • PTFE Sealing
    • PTFE Rod Stoppers and Caps

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Contributing Authors


Written by

Dr. Shadeepa Karunarathne

Product Development Electrochemist

Videography by

Sam Force

Graphic Designer